• 医薬GC血液
  • GLC Application

GHB

1. GBL 2. AMGBL

Columns SH-BAC Plus 1, 30m, 0.32mm ID, 1.80μm (P/N: 227-36260-01) Vial Pressure 30 psi
Injection headspace-loop split (split ratio 10:1) Pressurize Time 2 min
Liner 1 mm straight inlet liner Loop Pressure 20 psi
Inj. Port Temp. 200℃ Loop Fill Time 1 min
Instrument Tekmar HT3 Oven Temp. 80℃ (hold 0 min) to 180℃ at 10℃/min (hold 0 min)
Inj. Time 1 min Carrier Gas He, constant flow
Transfer Line Temp. 125℃ Linear Velocity 48 cm/sec
Valve Oven Temp. 125℃ Detector FID @ 240℃
Sample Temp. 100℃ Make-up Gas Flow Rate 30 mL/min
Sample Equil. Time 10 min Make-up Gas Type N2

【出典】株式会社島津製作所SHシリーズアプリデータ集 (株式会社島津ジーエルシー発行)

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