SHシリーズ
吸引剤分析
Inhalants
-
Peaks BAC Plus 1
tR (min)BAC Plus 2
tR (min)1. Methanol 1.340 1.230 2. Ethanol 1.694 1.470 3. Isopropanol 2.072 1.660 4. Diethyl ether 2.149 1.334 5. Acetone 2.256 1.589 6. Methylene chloride 2.405 1.703 7. MTBE 3.185 1.660 8. Hexane 3.683 1.660 9. Chloroform 3.956 2.667 10. MEK 4.210 2.543 -
Peaks BAC Plus 1
tR (min)BAC Plus 2
tR (min)11. Ethyl acetate 4.524 2.414 12. Benzene 5.390 2.883 13. Trichloroethylene 6.306 3.522 14. MIBK 8.101 5.775 15. Toluene 8.162 5.440 16. Ethylbenzene 10.286 7.681 17. m-Xylene 10.487 7.879 18. p-Xylene 10.487 7.879 19. o-Xylene 10.990 8.467
| Columns | SH-BAC Plus 1 30m, 0.32mm ID, 1.80μm (P/N: 227-36260-01) and SH-BAC Plus 2 30m, 0.32mm ID, 0.60μm (P/N: 227-36263-01) using SH-I Guard Column (P/N: 227-36305-01) with universal “Y” Press-Tight® connector |
Sample Equil. Time | 5 min |
|---|---|---|---|
| Diluent | Water | Vial Pressure | 30 psi |
| Conc. | 50 μg/mL each inhalant | Pressurize Time | 2 min |
| Injection | headspace-loop split (split ratio 50:1) | Loop Pressure | 20 psi |
| Liner | 1 mm straight inlet liner | Loop Fill Time | 1 min |
| Inj. Port Temp. | 220℃ | Oven Temp. | 40℃ (hold 4 min) to 120℃ at 10℃/min (hold 0 min) |
| Instrument | Tekmar HT3 | Carrier Gas | He, constant flow |
| Inj. Time | 3 min | Linear Velocity | 50 cm/sec |
| Transfer Line Temp. | 125℃ | Detector | FID @ 240℃ |
| Valve Oven Temp. | 125℃ | Make-up Gas Flow Rate | 30 mL/min |
| Sample Temp. | 70℃ | Make-up Gas Type | N2 |
【出典】株式会社島津製作所SHシリーズアプリデータ集 (株式会社島津ジーエルシー発行)
