酸性・中性薬物分析

Acidic/Neutral Drugs

  • 医薬GCMS薬物・毒物
  • GLC Application

酸性・中性薬物分析

1. Methprylon 2. Butalbital 3. Amobarbital 4. Meprobamate 5. Glutethimide 6. Phenobarbital 7. Methaqualone 8. Primidone

Column SH-I-5MS, 30m, 0.25mm ID, 0.25μm (P/N: 221-75940-30) Linear Velocity 30 cm/sec
Diluent methanol Detector MS
Conc. 20 ng each compound on column Mode Scan
Inj. Vol. 1.0 μL split (split ratio 50:1) Transfer Line Temp. 300℃
Liner Siltek Gooseneck Splitless (4mm) Analyzer Type Quadrupole
Inj. Temp. 250℃ Tune Type PFTBA
Oven Temp. 100℃ to 220℃at 15℃/min to 330℃ @ 10℃/min (hold 5 min) Ionization Mode EI
Carrier Gas He, constant pressure Scan Range 35-550 amu

【出典】株式会社島津製作所SHシリーズアプリデータ集(株式会社島津ジーエルシー発行)

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