SHシリーズ
抗ヒスタミン薬《未誘導体化》分析
Underivatized Antihistamines《Basic Drugs》
1. Phenylpropanolamine | 2. Ephedrine | 3. Pseudoephedrine | 4. Pheniramine | 5. Diphenhydramine | 6. Doxylamine |
7. Phenyltoloxamine | 8. Methapyrilene | 9. Chlorpheniramine | 10. Brompheniramine | 11. Triprolidine |
Column | SH-5 Amine, 30m, 0.32mm ID, 1.00μm (P/N: 227-36332-02) | Oven Temp. | 130℃ (hold 5 min) to 305℃ @10℃/min (hold 5 min) |
---|---|---|---|
Diluent | Antihistamines | Carrier Gas | H2, constant pressure |
Conc. | 1000 ng/μL | Linear Velocity | 43 cm/sec @ 130℃ |
Inj. Vol. | 1 μL split (split ratio 50:1) | Detector | FID @ 305℃ |
Inj. Temp. | 305℃ | FID sensitivity | 6.4 x 10-11 AFS |
【出典】株式会社島津製作所SHシリーズアプリデータ集(株式会社島津ジーエルシー発行)