• 医薬GCMS薬物・毒物
  • GLC Application

ベンゾジアゼピン分析

1. Oxazepam 2. Lorazepam 3. Diazepam 4. Flunitrazepam 5. Prazepam 6. Clonazepam 7. Alprazolam

Column SH-I-5Sil MS, 30m, 0.25mm ID, 0.25μm (P/N: 221-75954-30) Mode Scan
Diluent Butyl chloride Transfer Line Temp. 280℃
Conc. 15 μg/mL Analyzer Type Quadrupole
Inj. Vol. 1 μL splitless (hold 1 min) Source Temp. 200℃
Liner 3.5 mm taper splitless w/wool Electron Energy 70 eV
Inj. Temp. 280℃ Solvent Delay Time 4 min
Purge Flow 32.2 (20:1 split) mL/min Tune Type PFTBA
Oven Temp. 200℃ to 330℃ @ 15℃/min (hold 3 min) Ionization Mode EI
Carrier Gas He, constant linear velocity Scan Range 50-350 amu
Linear Velocity 50 cm/sec, 23.7 psi, 163.4 kPa @ 200℃ Scan Rate 5 scans/sec
Detector MS Instrument Shimadzu 2010 GC & QP2010+ MS

【出典】株式会社島津製作所SHシリーズアプリデータ集(株式会社島津ジーエルシー発行)

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