SHシリーズ
ベンゾジアゼピン分析
Benzodiazepines
1. Oxazepam 2. Lorazepam 3. Diazepam 4. Flunitrazepam 5. Prazepam 6. Clonazepam 7. Alprazolam
| Column | SH-I-5Sil MS, 30m, 0.25mm ID, 0.25μm (P/N: 221-75954-30) | Mode | Scan |
|---|---|---|---|
| Diluent | Butyl chloride | Transfer Line Temp. | 280℃ |
| Conc. | 15 μg/mL | Analyzer Type | Quadrupole |
| Inj. Vol. | 1 μL splitless (hold 1 min) | Source Temp. | 200℃ |
| Liner | 3.5 mm taper splitless w/wool | Electron Energy | 70 eV |
| Inj. Temp. | 280℃ | Solvent Delay Time | 4 min |
| Purge Flow | 32.2 (20:1 split) mL/min | Tune Type | PFTBA |
| Oven Temp. | 200℃ to 330℃ @ 15℃/min (hold 3 min) | Ionization Mode | EI |
| Carrier Gas | He, constant linear velocity | Scan Range | 50-350 amu |
| Linear Velocity | 50 cm/sec, 23.7 psi, 163.4 kPa @ 200℃ | Scan Rate | 5 scans/sec |
| Detector | MS | Instrument | Shimadzu 2010 GC & QP2010+ MS |
【出典】株式会社島津製作所SHシリーズアプリデータ集（株式会社島津ジーエルシー発行）
