SHシリーズ
薬物分析
Acidic/Neutral Drugs
1. Methprylon 2. Butalbital 3. Amobarbital 4. Meprobamate 5. Glutethimide 6. Phenobarbital 7. Methaqualone 8. Primidone
| Column | SH-I-5MS, 30m, 0.25mm ID, 0.25μm (P/N: 221-75940-30) | Carrier Gas | He, constant pressure |
|---|---|---|---|
| Sample | 1000μg/mL each | Linear Velocity | 30 cm/sec |
| Diluen | methanol | Detector | MS |
| Conc. | 20 ng each compound on column | Mode | Scan |
| Inj. Vol. | 1.0 μL split (split ratio 50:1) | Transfer Line Temp. | 300℃ |
| Liner | Siltek Gooseneck Splitless (4mm) | Analyzer Type | Quadrupole |
| Inj. Temp. | 250℃ | Tune Type | PFTBA |
| Oven Temp. | 100℃ to 220℃ @ 15℃/min to 330℃ @ 10℃/min (hold 5 min) | Ionization Mode | EI |
【出典】株式会社島津製作所SHシリーズアプリデータ集（株式会社島津ジーエルシー発行）
