SHシリーズ
遺伝毒性不純物分析 ハロゲン化アルキル
Genotoxic Impurities; Alkyl Halides
| Peaks | tR (min) | Peaks | tR (min) |
|---|---|---|---|
| 1. 2-Chloropropane | 2.10 | 4. 2-Bromopropane | 3.393 |
| 2. Bromoethane | 2.36 | 5. Butyl chloride | 4.627 |
| 3. 1-Chloropropane | 2.72 | 6. 1-Bromobutane | 5.973 |
| Column | SH-I-624Sil MS, 20m, 0.18mm ID, 1.00μm (P/N: 227-36075-01) | Mode | Scan |
|---|---|---|---|
| Diluent | DMSO | Transfer Line Temp. | 280℃ |
| Conc. | 1 μg/mL | Analyzer Type | Quadrupole |
| Inj. Vol. | 1 μL splitless (hold 0.5 min) | Source Temp. | 280℃ |
| Liner | 3.5 mm Single Gooseneck Liner with wool placed 3 cm from top (middle) | Solvent Delay Time | 0.5 min |
| Inj. Temp. | 220℃ | Ionization Mode | EI |
| Purge Flow | 3 mL/min | Scan Range | 30-300 amu |
| Oven Temp. | 40℃ (hold 3 min) to 200℃ @ 20℃/min | Scan Rate | 5 scans/sec |
| Carrier Gas | He, constant flow | Instrument | Shimadzu 2010 GC & QP2010+ MS |
| Linear Velocity | 40 cm/sec | Notes | Ions displayed: 42, 43, 57, 108 m/z |
| Detector | MS |
【出典】株式会社島津製作所SHシリーズアプリデータ集（株式会社島津ジーエルシー発行）
