香水（市販品）の分析

  • 香料GCMS匂い
  • GLC Application

香水（市販品）の分析

  • Peaks tR (min)
    1. Ethanol 4.18
    2. Linalool* 18.59
    3. Terpineol 21.21
    4. Benzyl acetate 21.78
    5. Citronellol* 22.29
    6. Dipropylene glycol isomer 1 23.31
    7. Geraniol* 23.57
  • Peaks tR (min)
    8. Dipropylene glycol isomer 2 24.10
    9. Dipropylene glycol isomer 3 24.20
    10. Lilial* 26.63
    11. Isoeugenol* 28.29
    12. Piperonal 29.20
    13. Diethyl phthalate 30.91
    14. Benzyl salicylate* 35.81

* Denotes fragrance allergen or suspected allergen

Column SH-PolarWax-MS, 30 m, 0.25 mm ID, 0.25 μm
(P/N: 227-36322-01)		 Scan Program Group Start Time
(min)		 Scan Range
(amu)		 Scan Rate
(scans/sec)
Conc. Neat 1 0 40-550 2
Inj. Vol. 1 μL split (split ratio 200:1) Transfer Line Temp. 260℃
Liner Premium 3.5 mm ID single taper w/wool Analyzer Type Quadrupole
Inj. Temp. 250℃ Source Temp. 250℃
Oven Temp. 35℃ (hold 5 min) to 250℃ at 7℃/min (hold 5 min) Electron Energy 70 eV
Carrier Gas He, constant linear velocity Solvent Delay Time 0.5 min
Linear Velocity 36 cm/sec Ionization Mode EI
Detector MS Instrument Shimadzu 2010 GC & QP2010+ MS
Mode Scan

【出典】株式会社島津製作所SHシリーズアプリデータ集 (株式会社島津ジーエルシー発行)

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