揮発性有機化合物③

Volatile Organic Compounds

  • 環境GCMSVOC
  • GLC Application

揮発性有機化合物③

1. dichlorodifl uoromethane 2. chloromethane 3. vinyl chloride 4. bromomethane 5. chloroethane
6. trichlorofl uoromethane 7. 1,1-dichloroethene 8. carbon disulfi de 9. 1,1,2-trichloro-1,2,2-trifl uoroethane 10. methylene chloride
11. acetone 12. trans-1,2-dichloroethene 13. methyl acetate 14. methyl tert-butyl ether 15. 1,1-dichloroethane
16. cis-1,2-dichoroethane 17. cyclohexane 18. bromochloromethane (IS) 19. chloroform 20. carbon tetrachloride
21. 1,1,1-trichloroethane 22. Propachlor 23. benzene 24. Cycloate 25. 1,2-dichloroethane
26. methylcyclohexane 27. trichloroethene 28. 1,4-difl uorobenzene (IS) 29. 1,2-dichloropropane 30. bromodichloromethane
31. cis-1,3-dichloropropene 32. toluene d8 (SS) 33. toluene 34. tetrachloroethane 35. 4-methyl-2-pentanone
36. trans-1,3-dichloropropane 37. 1,1,2-trichloroethane 38. dibromochloromethane 39. 1,2-dibromoethane 40. 2-hexanone
41. chlorobenzene d5 (IS) 42. chlorobenzene 43. ethylbenzene 44. m-xylene 45. p-xylene
46. o-xylene 47. styrene 48. bromoform 49. isopropylbenzene 50. 4-bromofl uorobenzene (SS)
51. 1,1,2,2-tetrachloroethane 52. 1,3-dichlorobenzene 53. 1,4-dichlorobenzene 54. 1,2-dichlorobenzene 55. 1,2-dibromo-3-chloropropane
56. 1,2,4-trichlorobenzene
Column SH-VMS, 30 m, 0.25 mm ID, 1.40 μm (P/N: 227-36268-01) Inj. Split (split ratio: 35:1)
Purge and Trap Trap:#10 (Tenax®/silica gel/carbon molecular sieve) Inj. Temp 200℃
Sample Temp:ambient Carrier Gas He, linear velocity 34 cm/sec., 40℃, constant flow
Purge:11 min @ 40 mL/min Oven Temp 40℃ (hold 4 min) to 90℃ @16 °C/min to 220℃ at 32℃/min (hold 5 min)
Desorb preheat:185℃ Detector MS
Desorb:0.5 min @ 190℃ Transfer Line Temp: 150 °C
Desorb flow rate:35.0 mL/mi Scan Range: 35-300 amu.
Bake:8 min @ 210℃ Ionization: EI
Interface:split injector
Transfer Line Temp:150℃

【出典】株式会社島津製作所SHシリーズアプリデータ集 (株式会社島津ジーエルシー発行)

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