SHシリーズ
揮発性有機化合物①
Semivolatiles
| 1. Isophorone | 2. 2-Nitro-m-xylene (SS) | 3. Naphthalene | 4. Dichlorvos (DDVP) | 5. Hexachlorocyclopentadiene |
| 6. EPTC | 7. Mevinphos | 8. Butylate | 9. Vernolate | 10. Dimethyl phthalate |
| 11. Pebulate | 12. Etridiazole | 13. 2,6-Dinitrotoluene | 14. Acenaphthylene | 15. Acenaphthene-d10 (IS) |
| 16. Chloroneb | 17. Tebuthiuron | 18. 2,4-Dinitrotoluene | 19. Molinate | 20. Diethyl phthalate |
| 21. Fluorene | 22. Propachlor | 23. Ethoprop (ethoprophos) | 24. Cycloate | 25. Chlorpropham |
| 26. Trifluralin | 27. Atraton | 28. Hexachlorobenzene | 29. Prometon | 30. Simazine |
| 31. Atrazine | 32. Propazine | 33. Pentachlorophenol | 34. Terbufos | 35. Propyzamide |
| 36. Diazinon | 37. Phenanthrene-d10 (IS) | 38. Phenanthrene | 39. Disulfoton | 40. Methylparaoxon |
| 41. Anthracene | 42. Terbacil | 43. Chlorothalonil | 44. Metribuzin | 45. Simetryn |
| 46. Ametryn | 47. Alachlor | 48. Prometryn | 49. Terbutryn | 50. di-n-Butyl phthalate |
| 51. Bromacil | 52. Cyanazine (Bladex) | 53. Metolachlor | 54. Chlorpyrifos | 55. Triadimefon |
| 56. DCPA methyl ester (Chlorthal-dimethyl) | 57. MGK-264 (isomer A) | 58. Diphenamid | 59. MGK-264 (isomer B) | 60. Merphos |
| 61. Heptachlor epoxide | 62. Fluoranthene | 63. Stirofos | 64. Disulfoton sulfone | 65. Butachlor |
| 66. Pyrene-d10 (SS) | 67. Fenamiphos | 68. Pyrene | 69. Napropamide (Devrinol) | 70. trans-Nonachlor |
| 71. Merphos oxide | 72. Tricyclazole (Beam) | 73. Carboxin | 74. Chlorobenzilate | 75. Benzyl butyl phthalate |
| 76. Norflurazon | 77. Bis(2-ethylhexyl) adipate | 78. Hexazinon (Velpar) | 79. Triphenylphosphate (SS) | 80. Benz[a]anthracene |
| 81. Chrysene-d12 (IS) | 82. Chrysene | 83. Bis(2-ethylhexyl) phthalate | 84. Fenarimol | 85. cis-Permethrin |
| 86. trans-Permethrin | 87. Di-n-octyl phthalate | 88. Benzo[b]fluoranthene | 89. Benzo[k]fluoranthene | 90. Benzo[a]pyrene |
| 91. Fluridone (Sonar) | 92. Perylene-d12 (SS) | 93. Indeno[1,2,3-cd]pyrene | 94. Dibenzo[a,h]anthracene | 95. Benzo[ghi]perylene |
| Column | SH-I-5MS, 30m, 0.25mm ID, 0.25μm (P/N: 221-75940-30) | Det. | MS |
|---|---|---|---|
| Inj. | 1.0 μL pulsed splitless injection: 50 psi (0.3 min.), 80 mL/min. (0.15 min.), gas saver 15 mL/min.(1min.), 4 mm Drilled Uniliner® inlet liner, hole near bottom |
Interface line temp. | 280℃ |
| Inj. temp. | 250℃ | Scan range | 35-550amu |
| Carrier gas | He, constant flow | Solvent delay | 3.00 min |
| Flow rate | 1.2 mL/min | Tune | DFTPP |
| Oven temp. | 90℃ (1 min) to 270℃ @ 20℃/min to 315℃ @ 6℃/min | Ionization | EI |
【出典】株式会社島津製作所SHシリーズアプリデータ集 (株式会社島津ジーエルシー発行)
