SHシリーズ
農薬分析①
Pesticldes
| 1. 2-Fluorophenol (SS) | 2. Phenol-d6 (SS) | 3. 1,4-Dichlorobenzene-d4 (IS) | 4. Nitrobenzene-d5 (SS) | 5. Naphthalene-d8 (IS) | 6. EPTC |
| 7. 2-Fluorobiphenyl (SS) | 8. Acenaphthene-d10 (IS) | 9. Propachlor | 10. Desisopropylatrazine | 11. Desethyl-atrazine | 12. 2,4,6-Tribromophenol (SS) |
| 13. Ethalfluralin | 14. Trifluralin | 15. Phorate | 16. Simazine | 17. Prometon | 18. Atrazine |
| 19. Propazine | 20. Terbufos | 21. Fonofos | 22. Phenanthrene-d10 (IS) | 23. Triallate | 24. Metribuzin |
| 25. Dimethenamid | 26. Acetochlor | 27. Alachlor | 28. Cyanazine | 29. Metolachlor | 30. Chlorpyrifos |
| 31. Pendimethalin | 32. p-Terphenyl-d14 (SS) | 33. Chrysene-d12 (IS) | 34. Perylene-d12 (IS) |
| Column | SH-I-1MS, 30m, 0.25mm ID, 0.25μm (P/N:221-75923-30) | Detector | MS |
|---|---|---|---|
| Inj. Vol. | 1.0 μL split (split ratio 10:1) | Mode | Scan |
| Liner | Drilled Uniliner (hole near bottom) | Transfer Line Temp. | 280℃ |
| Inj. Temp. | 250℃ | Solvent Delay Time | 2.5 min |
| Split Vent Flow Rate | 35 mL/min | Tune Type | DFTPP |
| Oven Temp. | 70℃ (hold 1 min) to 180℃ @ 20℃/min to 230℃ @ 5℃min to 325℃ @ 40℃/min (hold 3.5 min) |
Ionization Mode | EI |
| Carrier Gas | He, constant flow | Scan Range | 35-550 amu |
| Flow Rate | 1.2 mL/min |
【出典】株式会社島津製作所SHシリーズアプリデータ集 (株式会社島津ジーエルシー発行)
